Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Glycerol | HCID 753 | — |
| Reactant | HCID 70507109 | HCID 70507109 | — |
| Product | HCID 70506550 | HCID 70506550 | — |
Reaction Steps
A mixture of 2.25 g. of methyl 3-(4-tetradecenylamino)phenylbutyrate, 280 mg. of glycerol, and 1.37 g. of p-touluenesulfonic acid is heated at 180° C. for 18 hours and then is partitioned between ether and 3% aqueous sodium carbonate solution. The ether layer is separated, dried, and evaporated to yield the product as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04440940 |
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| Source dataset | uspto-grants-1984_04 |
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| ORD ID | ord-997f2b9ea3be40d089a02ce41988bc87 |
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| Source note | uspto-grants-1984_04 |
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