HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanol → HCID 86739351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | 2-ethylhexanoic acid tin(II) salt | HCID 9318 | — |
| Reactant | Dioxanone | HCID 18233 | — |
| Reactant | HCID 11815872 | HCID 11815872 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86739351 | HCID 86739351 | — |
Reaction Steps
p-Dioxanone (12.8 g, 0.125 moles), 3-methyl-2,5- morpholinedione (0.5 g, 0.00388 moles), 1-dodecanol (0.0369 g, 0.000198 moles), and a catalytic amount of stannous octoate (0.025 ml of a 0.33 M toluene solution, 0.0000083 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampoule according to the following temperature/time scheme:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04441496 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-4c9a86d310894dbca2769c6e71dfebd8 |
| Source note | uspto-grants-1984_04 |