HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanol → HCID 86739352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanol | HCID 8193 | — |
| Reactant | 2-ethylhexanoic acid tin(II) salt | HCID 9318 | — |
| Reactant | Dioxanone | HCID 18233 | — |
| Reactant | HCID 20463711 | HCID 20463711 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86739352 | HCID 86739352 | — |
Reaction Steps
p-Dioxanone (28.5 g, 0.279 moles), N-methyl-2,5- morpholinedione (1.5 g, 0.01162 moles), 1-dodecanol (0.082 g, 0.00044 moles), and a catalytic amount of stannous octoate (0.06 ml of a 0.33 M toluene solution, 0.0000198 moles) are heated and magnetically mixed in a flame and vacuum dried, sealed glass ampule according to the following temperature/time scheme:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04441496 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-6fc0e53c921340e78ed1e0e606cff725 |
| Source note | uspto-grants-1984_04 |