HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13457820, compound → HCID 23322143, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13457820 | HCID 13457820 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23322143 | HCID 23322143 | — |
Reaction Steps
9 g of the 2-dipropylamino-6-methoxy-7-nitro-1,2,3,4-tetrahydronaphthalene obtained in accordance with Example 1(b) are introduced into 200 ml of ethanol, together with 1 g of Raney nickel. At ambient temperature, hydrogenation is carried out under pressure until the absorption has stopped. After evaporation of the solvent, an oil remains which is shown to oxidise fairly readily in air.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442126 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-65641c9e69e64fafad009c26959a3ab8 |
| Source note | uspto-grants-1984_04 |