HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4-Benzyloxybenzoylchloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-(Benzyloxy)benzoic acid | HCID 73880 | — |
| Solvent | Trichloroethylene | HCID 6575 | — |
| Product | 4-Benzyloxybenzoylchloride | HCID 3766410 | — |
Reaction Steps
A solution of 164.7 g 4-benzyloxybenzoic acid obtained in step (a) and 80 ml of thionyl chloride in 750 ml of trichloroethylene was refluxed with stirring for 3 hrs. The crystalline residue obtained after evaporation was recrystallized from petroleum ether b.p. 80°-110° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04442300 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-1f4a1844baf04466957b01d2accc73de |
| Source note | uspto-grants-1984_04 |