Sodium Hydroxide → HCID 23707410, compound

HRID 325855Notes

Reaction equation

HRID 325855 reaction equation
[O:1]=[C:2]1[C:11]2=[CH:12][CH:13]=[C:14]([C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)[C:9]3=[C:10]2[N:5]([CH2:6][CH2:7][CH2:8]3)[CH:4]=[C:3]1[C:21]([OH:23])=[O:22].[OH-].[Na+:25]>O>[O:1]=[C:2]1[C:11]2=[CH:12][CH:13]=[C:14]([C:15]3[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=3)[C:9]3=[C:10]2[N:5]([CH2:6][CH2:7][CH2:8]3)[CH:4]=[C:3]1[C:21]([O-:23])=[O:22].[Na+:25]

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 13345750HCID 13345750, compound

Product 1

HCID 23707410HCID 23707410, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A sample of 6,7-dihydro-1-oxo-8-phenyl-1H,5H-benzo[ij]quinolizine-2-carboxylic acid, 100 ml of water and 0.176 g of sodium hydroxide was heated to obtain solution, filtered, then lyophilized to provide fluffy white solid sodium 6,7-dihydro-1-oxo-8-phenyl-1H,5H-benzo[ij]quinolizine-2-carboxylate, m.p. 230°-231° C. Analysis: Calculated for C20H16NNaO3.1.5H2O: %C, 65.2; %H, 5.2; %N, 3.8; Found: %C, 65.1; %H, 4.8; %N, 3.6. The structural assignment was confirmed by infrared spectral analysis.

Workup

  1. customto obtain solution
  2. filtrationfiltered

Sources & evidence

ORD record
ord-3bc382c11b8d4b81b984466203176942
Source dataset
uspto-grants-1984_04
Patent number
US04443447

Reaction notes

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