Sodium Hydroxide → HCID 23707410, compound

Participants

Reaction Steps

A sample of 6,7-dihydro-1-oxo-8-phenyl-1H,5H-benzo[ij]quinolizine-2-carboxylic acid, 100 ml of water and 0.176 g of sodium hydroxide was heated to obtain solution, filtered, then lyophilized to provide fluffy white solid sodium 6,7-dihydro-1-oxo-8-phenyl-1H,5H-benzo[ij]quinolizine-2-carboxylate, m.p. 230°-231° C. Analysis: Calculated for C20H16NNaO3.1.5H2O: %C, 65.2; %H, 5.2; %N, 3.8; Found: %C, 65.1; %H, 4.8; %N, 3.6. The structural assignment was confirmed by infrared spectral analysis.

Provenance & Evidence