HuagongsheHuagongshe Chemistry Print Report · For research reference only
Caprolactam → HCID 12833262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Caprolactam | HCID 7768 | — |
| Reactant | 1-Bromoheptane | HCID 12369 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | HCID 12833262 | HCID 12833262 | 90% |
Reaction Steps
Following example 10, 10.2 g of 50% sodium hydride-mineral oil dispersion (5.1 g of NaH, 0.2125 M), 20 g (0.177 M) of azacycloheptan-2-one and 35.8 g (0.2 M) of 1-bromoheptane on 18 hr. reflux gave 33.5 g (90%) of colorless product; b.p. 155°-158°/0.5 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444762 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-26afcd6002fe42a9a3a409972f066a9e |
| Source note | uspto-grants-1984_04 |