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HRID326105

反应详情

EQUATION

反应方程式

HRID 326105 的结构方程式

REACTANTS

反应物

3
结构：CCCCCCCCCCCCCCCBr
HCID12394

1-Bromopentadecane

C15H31Br

结构：CCOC(=O)CCS
HCID21625

Ethyl 3-mercaptopropionate

C5H10O2S

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCCCCSCCCO
HCID20462062

未命名化合物

收率 84%

PROCEDURE

实验过程

1-Bromopentadecane is reacted in the usual way with ethyl β-mercaptopropionate and the syrup obtained reduced with lithium aluminium hydride to give a yield of 84% of theory of 3-pentadecylthiopropanol; m.p. 36°-39° C.

WORKUP

后处理

  1. customthe syrup obtained