HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromopentadecane → 3-Pentadecylthiopropanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromopentadecane | HCID 12394 | — |
| Reactant | Ethyl 3-mercaptopropionate | HCID 21625 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 3-Pentadecylthiopropanol | HCID 20462062 | 84% |
Reaction Steps
1-Bromopentadecane is reacted in the usual way with ethyl β-mercaptopropionate and the syrup obtained reduced with lithium aluminium hydride to give a yield of 84% of theory of 3-pentadecylthiopropanol; m.p. 36°-39° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04444766 |
| Source dataset | uspto-grants-1984_04 |
| ORD ID | ord-b31fba29f7574ee6a1a36ee713ddad8d |
| Source note | uspto-grants-1984_04 |