Potassium Iodide → HCID 19092082, compound

HRID 326246Notes

Reaction equation

HRID 326246 reaction equation
Br[CH2:2][CH2:3][C:4]1[CH:14]=[CH:13][C:7]2[NH:8][C:9](=[O:12])[CH2:10][O:11][C:6]=2[CH:5]=1.[I-].[K+].C[N:18](C)C=O>>[NH2:18][CH2:2][CH2:3][C:4]1[CH:14]=[CH:13][C:7]2[NH:8][C:9](=[O:12])[CH2:10][O:11][C:6]=2[CH:5]=1

Participants

4

Reactant 3

HCID 4875Potassium IodideHCID 6228DimethylformamideHCID 19092046HCID 19092046, compound

Product 1

HCID 19092082HCID 19092082, compound

Procedure

In a 250-cm3 ground-necked flask, 0.01 mol of 7-(2-bromoethyl)-3-oxo-2,3-dihydro-1,4-benzoxazine and 0.3 g of potassium iodide are dissolved in 30 cm3 of dimethylformamide.

Sources & evidence

ORD record
ord-ee0de7c8c52d479fb60fbd436f869bb7
Source dataset
uspto-grants-1993_12
Patent number
US05268381

Reaction notes

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