HCID 22849140, compound → HCID 22849139, compound

Participants

Reaction Steps

The resultant compound from Example 137 (1.00 mmol) was stirred for 1 h in 4M HCl/ethanol. The mixture was evaporated and the residue was dissolved in water which was made basic with solid K2CO3 and was then saturated with NaCl. The mixture was extracted with chloroform which was dried over Na2SO4 and evaporated to afford the desired product.

Provenance & Evidence