HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14629903, compound → HCID 14629908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14629903 | HCID 14629903 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14629908 | HCID 14629908 | 99.4% |
Reaction Steps
A solution of 700 mg of the product from Example 177 in 10 ml of methanol was stirred vigorously under a hydrogen atmosphere using 10% Pd/C as catalyst. After 30 min, the catalyst was filtered off and the solution concentrated to give 470 mg the desired product. Mass spectrum: M+ =279.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05268374 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-a6181ea709bb466aaddded53449fe280 |
| Source note | uspto-grants-1993_12 |