HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus tribromide → HCID 14480083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus tribromide | HCID 24614 | — |
| Reactant | HCID 14480065 | HCID 14480065 | — |
| Catalyst | Pyridine | HCID 1049 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 14480083 | HCID 14480083 | — |
Reaction Steps
A mixture of 5 g of 2,5,8-heptadecatriyn-1-ol, one drop of pyridine and 2 g of phosphorus tribromide in 20 cm3 of ethyl ether is heated under reflux for 3 hours. The ether phase is then washed initially with sodium bicarbonate and then with water, and then dried over magnesium sulphate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05268494 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-17329ed6b16647f19989ba67d68f68e2 |
| Source note | uspto-grants-1993_12 |