HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Iodopropane → 2-Chloro-5-(propane-1-sulfonyl)-benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | 2-Chloro-5-(methylsulphonyl)benzoic acid | HCID 2329132 | — |
| Reactant | 2-Chloro-5-sulfino-benzoic acid | HCID 15112904 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | 2-Chloro-5-(propane-1-sulfonyl)-benzoic acid | HCID 43141000 | 3% |
Reaction Steps
The title compound was synthesised according to the procedure described for the synthesis of 2-Chloro-5-methanesulfonyl-benzoic acid from 2-Chloro-5-sulfino-benzoic acid and 1-iodopropane in 20 ml propanol/20 ml water and obtained in 3% yield. MS (m/e): 261.1 (MH−, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07427612B2 |
| Source dataset | uspto-grants-2008_09 |
| ORD ID | ord-ed83c1a300cb49fd8b0b7ca414a18e3f |
| Source note | uspto-grants-2008_09 |