HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,6-Dichloro-3-oxoindan-1-carbonyl chloride → 4-(5,6-Dichloro-3-oxoindan-1-carbonyl)-3-(morpholinomethyl)morpholine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,6-Dichloro-3-oxoindan-1-carbonyl chloride | HCID 15132407 | — |
| Reactant | 3-(Morpholinomethyl)morpholine | HCID 18915099 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 4-(5,6-Dichloro-3-oxoindan-1-carbonyl)-3-(morpholinomethyl)morpholine hydrochloride | HCID 18915127 | 73.9% |
Reaction Steps
The procedure described in Example 24 was repeated, but using 1.25 g of 3-(morpholinomethyl)morpholine, 2.67 ml of triethylamine and 1.11 g of 5,6-dichloro-3-oxoindan-1-carbonyl chloride, to afford 0.7 g of the title compound, melting at 210°-216° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270327 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-88195629b6284286a46f571c9a3d93e8 |
| Source note | uspto-grants-1993_12 |