HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Pyrrolidin-1-ylmethyl)thiomorpholine → HCID 178479631, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Pyrrolidin-1-ylmethyl)thiomorpholine | HCID 15730147 | — |
| Reactant | 4,5-dihydro-6-oxo-6H-cyclopenta[b]thiophene-4-carbonyl chloride | HCID 18915019 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 178479631 | HCID 178479631 | 25.8% |
Reaction Steps
The procedure described in Example 24 was repeated, but using 0.96 g of 3-(pyrrolidin-1-ylmethyl)thiomorpholine, 1.39 ml of triethylamine and 1.0 g of 4,5-dihydro-6 oxo-6H-cyclopenta[b]thiophene-4-carbonyl chloride, to afford 0.5 g of the title compound, melting at 204°-223° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270327 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-6d5a8254218c489c908a79801091f2fb |
| Source note | uspto-grants-1993_12 |