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HRID326777

反应详情

EQUATION

反应方程式

HRID 326777 的结构方程式

REACTANTS

反应物

2
结构：OCc1ccccc1
HCID244

Benzyl alcohol

C7H8O

结构：O=C1CCC(=O)O1
HCID7922

Succinic anhydride

C4H4O3

PRODUCTS

生成物

1
结构：O=C(O)CCC(=O)OCc1ccccc1
HCID8788

Benzylsuccinate

C11H12O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

A solution of succinic anhydride (16.0 g, 160 mmol) and benzyl alcohol (17.1 g, 158 mmol) in toluene (200 mL) was heated at reflux for 3.5 hr. At this time, the solvent was removed in vacuo to leave 3-(benzyloxycarbonyl)propanoic acid as a white solid.

WORKUP

后处理

  1. temperatureat reflux for 3.5 hr
  2. customAt this time, the solvent was removed in vacuo