HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 1-(Phenylmethyl) butanedioate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | Succinic anhydride | HCID 7922 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(Phenylmethyl) butanedioate | HCID 8788 | — |
Reaction Steps
A solution of succinic anhydride (16.0 g, 160 mmol) and benzyl alcohol (17.1 g, 158 mmol) in toluene (200 mL) was heated at reflux for 3.5 hr. At this time, the solvent was removed in vacuo to leave 3-(benzyloxycarbonyl)propanoic acid as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270331 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-1b403b4b104a431aa75f5feb592d3c25 |
| Source note | uspto-grants-1993_12 |