HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Benzyloxymethyl-4(3H)-pteridinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Amino-2-(benzyloxymethyl)pteridine | HCID 10778229 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 2-Benzyloxymethyl-4(3H)-pteridinone | HCID 135461697 | — |
Reaction Steps
Obtained using the procedure described in section b of Example 9, starting with 10.0 g (0.037 mole) of crude 4-amino-2-(benzyloxymethyl)pteridine in 300 ml of 5% aqueous sodium hydroxide. Heating time: 2 hours at 80° C. Yld: 8.2 g (83%), m.p. 157°-159° C. (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270465 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-61a7494901f54b37947756cbcfb90b9f |
| Source note | uspto-grants-1993_12 |