HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14880138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | (Methoxymethoxy)acetonitrile | HCID 19736216 | — |
| Product | HCID 14880138 | HCID 14880138 | — |
Reaction Steps
Obtained using the procedure described in section a of Example 2, starting with 286.8 g (2.84 moles) of methoxymethoxyacetonitrile [prepared according to D. J. Loder and W. M. Bruner, U.S. Pat. No. 2,398,757; C.A. 1946, 40, 3774] and 6.5 g (0.284 gram-atom) of sodium in 1430 ml of methanol. Reaction time: 2 days. Yld: 302.6 g (80%), b.p.15 62°-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270465 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-7d41e234c6214dbbbb2e4e714ad9efd2 |
| Source note | uspto-grants-1993_12 |