Methanol → HCID 14880138, compound

HRID 326840Notes

Reaction equation

HRID 326840 reaction equation
[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6]#[N:7].[Na].[CH3:9][OH:10]>>[CH3:1][O:2][CH2:3][O:4][CH2:5][C:6](=[NH:7])[O:10][CH3:9]

Participants

4

Reactant 3

HCID 887MethanolHCID 5360545SodiumHCID 19736216(Methoxymethoxy)acetonitrile

Product 1

HCID 14880138HCID 14880138, compound

Procedure

Obtained using the procedure described in section a of Example 2, starting with 286.8 g (2.84 moles) of methoxymethoxyacetonitrile [prepared according to D. J. Loder and W. M. Bruner, U.S. Pat. No. 2,398,757; C.A. 1946, 40, 3774] and 6.5 g (0.284 gram-atom) of sodium in 1430 ml of methanol. Reaction time: 2 days. Yld: 302.6 g (80%), b.p.15 62°-65° C.

Workup

  1. customObtained
  2. customprepared
  3. customReaction time
  4. custom2 days
  5. custom302.6 g (80%), b.p.15 62°-65° C.

Sources & evidence

ORD record
ord-7d41e234c6214dbbbb2e4e714ad9efd2
Source dataset
uspto-grants-1993_12
Patent number
US05270465

Reaction notes

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