HRID326843

反应详情

EQUATION

反应方程式

HRID 326843 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Obtained using the procedure described in section c of Example 2, starting with 8.8 g (0.073 mole) of 3-amino-2-pyrazinecarbonitrile and 13.0 g (0.11 mole) of 2-isopropoxyacetamidine in 295 ml of absolute ethanol. Refluxing time: 4 hours. Yld: 4.5 g (28%), m.p. 139°-141° C. (ethyl acetate).

WORKUP

后处理

  1. customObtained
  2. temperatureRefluxing time
  3. custom4 hours