HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Isopropoxymethyl-4(3H)-pteridinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 4-Amino-2-(isopropoxymethyl)pteridine | HCID 10513070 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 2-Isopropoxymethyl-4(3H)-pteridinone | HCID 135528322 | — |
Reaction Steps
Obtained using the procedure described in section d of Example 2, starting with 4.5 g (0.0205 mole) of 4-amino-2-(isopropoxymethyl)pteridine in 150 ml of 5% aqueous sodium hydroxide. Heating time: 2 hours at 80° C. Yld: 3.0 g (66%), m.p. 198°-199° C. (ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05270465 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-15c16d4e0c0b495d98afbcfc12788beb |
| Source note | uspto-grants-1993_12 |