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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 326862Generated: October 29, 2026

HCID 10850551, compound → HCID 135536693, compound

https://huagongshe.com/reaction/326862

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10850551HCID 10850551—
ReactantN,N-dimethylformamide ethanolHCID 19794673—
SolventSodium HydroxideHCID 14798—
ProductHCID 135536693HCID 135536693—

Reaction Steps

Obtained using the procedure described in section b of Example 9, starting with 5.4 g (0.019 mole) of 4-amino-2-(benzylthiomethyl)pteridine in 400 ml of 5% aqueous sodium hydroxide. Reaction time: 7 hours at 85° C. Yld: 1.7 g (31%), m.p. 224°-226° C. (ethanol/N,N-dimethylformamide).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05270465
Source datasetuspto-grants-1993_12
ORD IDord-00f4e5f422e0456fba690aeb591be7a3
Source noteuspto-grants-1993_12