HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14957731, compound → HCID 14957732, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14957731 | HCID 14957731 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 14957732 | HCID 14957732 | 0.1% |
Reaction Steps
To a solution of 0.15 g (0.51 mol) of the product obtained in example 50 in 9 mL ethyl acetate, were added 0.03 g of 5% Pd/C and the mixture was hydrogenated at atmospheric pressure for 2 h. After filtration, the solvent was removed, affording 0.110 g of the title compound of this example as a white solid (yield: 74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05272170 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-d91ec63109f64e4d8a62cff91346d438 |
| Source note | uspto-grants-1993_12 |