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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 327138Generated: October 30, 2026

HCID 14957731, compound → HCID 14957732, compound

https://huagongshe.com/reaction/327138

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14957731HCID 14957731—
CatalystPalladiumHCID 23938—
SolventEthyl AcetateHCID 8857—
ProductHCID 14957732HCID 149577320.1%

Reaction Steps

To a solution of 0.15 g (0.51 mol) of the product obtained in example 50 in 9 mL ethyl acetate, were added 0.03 g of 5% Pd/C and the mixture was hydrogenated at atmospheric pressure for 2 h. After filtration, the solvent was removed, affording 0.110 g of the title compound of this example as a white solid (yield: 74%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05272170
Source datasetuspto-grants-1993_12
ORD IDord-d91ec63109f64e4d8a62cff91346d438
Source noteuspto-grants-1993_12