HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 1360, compound → HCID 178492576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 1360 | HCID 1360 | — |
| Reactant | Methyl iodide | HCID 6328 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178492576 | HCID 178492576 | — |
Reaction Steps
Stir at room temperature for about 2.5 hours, 300 mg. of the compound prepared in Example 1, 5 ml. methylene chloride and 0.066 ml. methyl iodide. Elute on a coarse silica column with methylene chloride, then 5% methanol/methylene chloride and finally 10% methanol/methylene chloride, to isolate the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05272167 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-bd4e9426da714b9bbd5a3662ff897126 |
| Source note | uspto-grants-1993_12 |