Dichloromethane → HCID 22849453, compound

HRID 327341Notes

Reaction equation

HRID 327341 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:11]2[O:23][CH:12]2[C:13]2[CH:18]=[CH:17][C:16]([O:19][CH3:20])=[C:15]([O:21][CH3:22])[CH:14]=2)[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[CH3:24][O:25][CH:26]([O:29][CH3:30])[CH2:27][NH2:28].ClCCl>CC(O)CC>[CH3:22][O:21][C:15]1[CH:14]=[C:13]([C@H:12]([OH:23])[C@@H:11]([C:5]2[CH:6]=[CH:7][C:8]([O:9][CH3:10])=[C:3]([O:2][CH3:1])[CH:4]=2)[NH:28][CH2:27][CH:26]([O:29][CH3:30])[O:25][CH3:24])[CH:18]=[CH:17][C:16]=1[O:19][CH3:20]

Participants

5

Reactant 3

HCID 6344DichloromethaneHCID 89728Aminoacetaldehyde dimethyl acetalHCID 19734818HCID 19734818, compound

Product 1

HCID 22849453HCID 22849453, compound

Reagents, catalysts & solvents 1

HCID 6568(+-)-2-ButanolSolvent

Procedure

57 g (0.17 mol) of 3,3',4,4'-tetramethoxy-stilbene oxide, 120 ml (1.1 mol) of aminoacetaldehyde dimethyl acetal, 1.5 l of dichloromethane, 80 ml of 2-butanol.

Sources & evidence

ORD record
ord-b1f44f1594624956bb13a745659cb6ee
Source dataset
uspto-grants-1993_12
Patent number
US05272270

Reaction notes

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