HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl Peroxide → HCID 19023690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Chlorosuccinimide | HCID 31398 | — |
| Reactant | 1,8-Naphthyridine, 2-methyl- | HCID 74073 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 19023690 | HCID 19023690 | — |
Reaction Steps
A solution of 2-methyl-1,8-naphthyridine (Chem. Pharm. Bull., 19, 1857 (1971)), N-chlorosuccinimide (1.1 equivalent), and a catalytic amount of benzoylperoxide in CCl4 were irradiated at reflux with a 225 watt lamp for 5 hours. After cooling, the solid was filtered and the filtrate evaporated to dryness. The crude residue was chromatographed to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273980 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-2c2073870aab46df98688f83d3a807a3 |
| Source note | uspto-grants-1993_12 |