HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 178488033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 2-Amino-5-methoxyphenol Hydrochloride | HCID 12210184 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178488033 | HCID 178488033 | — |
Reaction Steps
2-amino-5-methoxyphenol hydrochloride (6 g) in 80 ml of water was stirred at room temperature while thiophosgene (3.92 g) was added dropwise as a solution in 30 ml of diethyl ether at a rate such that the resultant exotherm was controlled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273988 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-ff02c3cd9cb64793ac7d9337ff13711b |
| Source note | uspto-grants-1993_12 |