Potassium Carbonate → HCID 54050485, compound

Participants

Reaction Steps

2-Mercaptobenzoxazole (2 g), 4-bromo-1,1,2-trifluorobut-1-ene (2.75 g) and potassium carbonate (1 g) were stirred together in 40 ml of acetone and heated to reflux. After 2 hours the reaction mixture was allowed to cool, filtered to remove insoluble potassium salts and the filterate was evaporated under reduced pressure to yield 3.54 g of a brown oil which was used in step b without purification.

Provenance & Evidence