HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 178505460, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 2-Amino-5-fluorophenol | HCID 185763 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178505460 | HCID 178505460 | — |
Reaction Steps
2-Amino-5-fluorophenol [CAS:53981-24-1] (18.4 g) in 100 ml of water was stirred at room temperature while thiophosgene (16.8 g) was added dropwise as a solution in 100 ml of diethyl ether at such a rate that the resultant exotherm was controlled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273988 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-645dbbb60e834596b912c511d86f55e3 |
| Source note | uspto-grants-1993_12 |