O,O-Dipyridin-2-yl carbonothioate → HCID 19919467, compound

HRID 327466Notes

Reaction equation

HRID 327466 reaction equation
N1C=CC=CC=1OC(=S)OC1C=CC=CN=1.Cl[CH2:18][C:19]([NH:21][C:22]1[CH:23]=[CH:24][CH:25]=[C:26]2[C:31]=1[NH:30][CH2:29][CH:28]([N:32]([CH3:34])[CH3:33])[CH2:27]2)=[O:20]>CN(C=O)C>[CH3:33][N:32]([CH3:34])[CH:28]1[CH2:29][N:30]2[CH2:18][C:19](=[O:20])[NH:21][C:22]3[CH:23]=[CH:24][CH:25]=[C:26]([C:31]=32)[CH2:27]1

Participants

4

Reactant 2

HCID 719784O,O-Dipyridin-2-yl carbonothioateHCID 54046780HCID 54046780, compound

Product 1

HCID 19919467HCID 19919467, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

This compound was prepared using the procedure of Example 66, but substituting chloroacetic anhydride for di (2-pyridyl)thiocarbonate and cyclizing the initially formed N8 -(chloroacetyl)-1,2,3,4-tetrahydro-N3,N3 -dimethyl-3,8-quinolinediamine by heating at 150°0 C. in DMF.

Workup

  1. customThis compound was prepared
  2. temperatureby heating at 150°0 C

Sources & evidence

ORD record
ord-2bd28cd6a0614327be8018b870045071
Source dataset
uspto-grants-1993_12
Patent number
US05273975

Reaction notes

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