HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 11459998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | HCID 15291955 | HCID 15291955 | — |
| Product | HCID 11459998 | HCID 11459998 | — |
Reaction Steps
2-Chloro-5,6-dihydro-N,N-dipropyl-4H-imidazo(4,5,1-ij)quinolin-5-amine was refluxed in acetic acid for 1 hour. The solvent was removed and the residue was partitioned between ethyl acetate and sodium hydroxide solution. Evaporation of the ethyl acetate afforded 5-(dipropylamino)-5,6-dihydro-4H-imidazo(4,5,1-ij)quinoline-2(1H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273975 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-7937fc0ede174da9a189804e733b5833 |
| Source note | uspto-grants-1993_12 |