HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → HCID 18934809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | HCID 178418363 | HCID 178418363 | — |
| Product | HCID 18934809 | HCID 18934809 | 71.5% |
Reaction Steps
Using the procedure of Example 20, 2.0 g (5.96 mmol) of 4-mercapto-2-phenyl-pyrimidine-5-carboxylic acid phenethyl-amide were treated with 1.66 g (6.56 mmol) of iodine to give 1.42 g of the title compound after recrystallization from isopropanol, mp 144°-147° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05733921 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-156358fb63ab4966938ac93b299a8521 |
| Source note | uspto-grants-1998_03 |