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HRID327518

反应详情

EQUATION

反应方程式

HRID 327518 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CC(CNC(=O)OC(C)(C)C)C(=O)O
HCID4192640

3-[(tert-Butoxycarbonyl)amino]-2-methylpropanoic acid

C9H17NO4

结构：CC(C)(C)OC(=O)N[C@@H](CC(=O)OCc1ccccc1)C(N)=O
HCID10615806

未命名化合物

PRODUCTS

生成物

1
结构：CC(CNC(=O)OC(C)(C)C)C(=O)N[C@@H](CC(=O)OCc1ccccc1)C(N)=O
HCID86747430

未命名化合物

PROCEDURE

实验过程

Benzyl (S)-3-(1-t-butoxyformamido)succinamate was deprotected using trifluoroacetic acid and then coupled with DL-N-(t-butoxycarbonyl)-2-methyl-β-alanine to yield t-Butyl [(RS)-2-[[(S)-2-[(benzyloxy)carbonyl]-1-carbamoylethyl]-carbamoyl]propyl]carbamate, m.p. 135°-136° C.