Ethanol, 2-(o-tolyloxy)- → 2-(2-Methylphenoxy)ethanol sulfamate

HRID 327666Notes

Reaction equation

HRID 327666 reaction equation
[S:1](Cl)(=[O:4])(=[O:3])[NH2:2].[CH3:6][C:7]1[CH:16]=[CH:15][CH:14]=[CH:13][C:8]=1[O:9][CH2:10][CH2:11][OH:12]>>[S:1]([O:12][CH2:11][CH2:10][O:9][C:8]1[CH:13]=[CH:14][CH:15]=[CH:16][C:7]=1[CH3:6])(=[O:4])(=[O:3])[NH2:2]

Participants

3

Reactant 2

HCID 22539Ethanol, 2-(o-tolyloxy)-HCID 24499Chlorosulfamic acid

Product 1

HCID 191086612-(2-Methylphenoxy)ethanol sulfamateYield 53%

Procedure

The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(2-methylphenoxy)ethanol in 53% yield as an off-white solid, mp 81.5°-83° C.

Sources & evidence

ORD record
ord-f4add27b6d4b4a2eb0baaadd2b3736ff
Source dataset
uspto-grants-1993_12
Patent number
US05273993

Reaction notes

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