HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 2-(o-tolyloxy)- → 2-(2-Methylphenoxy)ethanol sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 2-(o-tolyloxy)- | HCID 22539 | — |
| Reactant | Chlorosulfamic acid | HCID 24499 | — |
| Product | 2-(2-Methylphenoxy)ethanol sulfamate | HCID 19108661 | 53% |
Reaction Steps
The title compound was prepared by procedures of Example 33 from sulfamoyl chloride and 2-(2-methylphenoxy)ethanol in 53% yield as an off-white solid, mp 81.5°-83° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-f4add27b6d4b4a2eb0baaadd2b3736ff |
| Source note | uspto-grants-1993_12 |