HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → 2-Fluorophenyl sulfamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 2-Fluorophenol | HCID 9707 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2-Fluorophenyl sulfamate | HCID 53908852 | 38.2% |
Reaction Steps
This compound was prepared according to the procedure of Example 56. A mixture of 11.2 g (0.1 mole) of 2-fluorophenol and 9.1 ml (14.8 g, 0.105 mole) of chlorosulfonyl isocyanate in 50 ml of toluene gave 7.3 g (38%) of the title compound as a white solid, mp 63°-64° (benzene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273993 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-e98fb441880b41db928d4d12bffe22b3 |
| Source note | uspto-grants-1993_12 |