Triethylamine → HCID 21201151, compound

Participants

Reaction Steps

To a suspension of N,N'-bis(1-oxo-3-chloropropyl)-ethanediamide (3.0 g; 11 mmol) in methylene chloride (40 ml), triethylamine (2.82 g; 28 mmol) was added, and the resultant mixture was stirred at room temperature for 2 hours. The precipitated solid was collected and washed with water to give N,N'-bis(1-oxo-2-propenyl)ethanediamide (0.1 g). Yield, 4.6%.

Provenance & Evidence