Hydrogen Bromide → HCID 18633023, compound

HRID 327911Notes

Reaction equation

HRID 327911 reaction equation
[CH2:1]([C:3]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[O:7][C:6](=[O:8])[C@H:5]([CH3:9])[O:4]1)[CH3:2].[BrH:16].BrBr>C(Cl)(Cl)(Cl)Cl>[Br:16][CH:1]([C:3]1([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=2)[O:7][C:6](=[O:8])[C@H:5]([CH3:9])[O:4]1)[CH3:2]

Participants

5

Reactant 3

HCID 260Hydrogen BromideHCID 24408BromineHCID 18633024HCID 18633024, compound

Product 1

HCID 18633023HCID 18633023, compound

Reagents, catalysts & solvents 1

HCID 5943Carbon TetrachlorideSolvent

Procedure

To a solution of 2-ethyl-2-phenyl-5(S)-methyl-1,3-dioxolane-4-one (1 mmol) and hydrogen bromide (0.1 mmol) in carbon tetrachloride (3 ml), bromine (1 mmol) was added and the temperature was kept at 15° C.

Workup

  1. customwas kept at 15° C.

Sources & evidence

ORD record
ord-b104248513fe410cb5b9f3a0b2f21777
Source dataset
uspto-grants-1993_12
Patent number
US05274186

Reaction notes

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