HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → 2-[(5-Bromopentyl)oxy]-5-[[4-(ethoxycarbonyl)phenyl]carbonyl]benzenepropanoic Acid Ethyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | HCID 53998721 | HCID 53998721 | — |
| Product | 2-[(5-Bromopentyl)oxy]-5-[[4-(ethoxycarbonyl)phenyl]carbonyl]benzenepropanoic Acid Ethyl Ester | HCID 53687280 | 72.6% |
Reaction Steps
Starting with 0.484 g (1.31 mmol) of 5-[[4-(ethoxycarbonyl)phenyl]carbonyl]-2-hydroxybenzenepropanoic acid ethyl ester, and 2.4 g (10.44 mmol) of 1,5-dibromopentane, the title compound was obtained in 72.6% yield as a white solid, mp 76.5°-78° C., using the procedure of example 21.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273999 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-901ad28685db4a7fa12f1619c01f85c2 |
| Source note | uspto-grants-1993_12 |