HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53952491, compound → HCID 19921959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53952491 | HCID 53952491 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 19921959 | HCID 19921959 | 52.6% |
Reaction Steps
Starting with 0.736 g (1.19 mmol) of 2-[[5-[(3,4-dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)oxy]pentyl]oxy]-6-(2-ethoxy-2oxoethoxy)-1-naphthalenepropanoic acid ethyl ester from the preceding example, the title compound (0.352 g; 52.6%) was obtained as a white solid, mp 160.5°-163° C. (recrystallized from hexane-ethyl acetate), using the procedure of example 226.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05273999 |
| Source dataset | uspto-grants-1993_12 |
| ORD ID | ord-d34c5424bb354c1582170b3e2c980699 |
| Source note | uspto-grants-1993_12 |