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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 328041Generated: October 29, 2026

HCID 53952491, compound → HCID 19921959, compound

https://huagongshe.com/reaction/328041

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53952491HCID 53952491—
SolventEthyl acetate hexaneHCID 21226206—
ProductHCID 19921959HCID 1992195952.6%

Reaction Steps

Starting with 0.736 g (1.19 mmol) of 2-[[5-[(3,4-dihydro-4-oxo-8-propyl-2H-1-benzopyran-7-yl)oxy]pentyl]oxy]-6-(2-ethoxy-2oxoethoxy)-1-naphthalenepropanoic acid ethyl ester from the preceding example, the title compound (0.352 g; 52.6%) was obtained as a white solid, mp 160.5°-163° C. (recrystallized from hexane-ethyl acetate), using the procedure of example 226.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05273999
Source datasetuspto-grants-1993_12
ORD IDord-d34c5424bb354c1582170b3e2c980699
Source noteuspto-grants-1993_12