HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 54358335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 13002188 | HCID 13002188 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54358335 | HCID 54358335 | — |
Reaction Steps
In a manner analogous to that given in Example 1 (b) but with ion-exchange in methanol, from the benzylamine salt of (1R)-1-[(N-benzyloxycarbonyl-L-alanyl)amino]-ethylphosphonic acid there was obtained (1R)-1-(L-alanylamino)-2-phenylethylphosphonic acid of melting point 250°-260° C (decomposition); [α]D20 = -40.3° (c = 0.21% in water).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016148 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-661646a7756d45baaa5a4915a3f72838 |
| Source note | uspto-grants-1977_04 |