HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 86734598, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 68117104 | HCID 68117104 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 86734598 | HCID 86734598 | — |
Reaction Steps
10 g of 4-(2-imidazolinyl)-phenylacetic acid (melting point 196° to 197° C) were stirred with 150 ml of anhydrous benzene and 90 ml of thionyl chloride for 5 hours at 50° to 60° C. After cooling, the crystalline product was filtered off with suction, washed with anhydrous benzene and dried under reduced pressure. 11 g of 4-(2-imidazolinyl)-phenyl-acetyl chloride-hydrochloride were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016159 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-7bb00787c4f744c3ae1a8d6e0c536b09 |
| Source note | uspto-grants-1977_04 |