HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aceton-methanol → 3-dimethylamino-11-methyl-1,3,4,14b-tetrahydro-2H-pyridino [1,2-d]-dibenzo[b,f](1,4)-oxazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aceton-methanol | HCID 21894497 | — |
| Reactant | 3-dimethylamino-7-trifluoromethyl-1,3,4,14b-tetrahydro-2H-pyridino[1,2-d]-dibenzo[b,f](1,4)-thiazepine | HCID 70637428 | — |
| Product | 3-dimethylamino-11-methyl-1,3,4,14b-tetrahydro-2H-pyridino [1,2-d]-dibenzo[b,f](1,4)-oxazepine | HCID 70637876 | — |
Reaction Steps
Rf in methanol:acetone (8:2) = 0.20 (equatorial). 3-dimethylamino-7-trifluoromethyl-1,3,4,14b-tetrahydro-2H-pyridino[ 1,2-d]-dibenzo[b,f](1,4)-thiazepine:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04016161 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-aefcbfa6dd4247baacbf836c92cfd0f5 |
| Source note | uspto-grants-1977_04 |