Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Epoxybutane → 1-(p-Ethylphenoxy)-butan-2-ol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Epoxybutane | HCID 7834 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | 4-Ethylphenol | HCID 31242 | — |
| 생성물 | 1-(p-Ethylphenoxy)-butan-2-ol | HCID 21444115 | 76.3% |
반응 단계
In a closed vessel 12.2g (0.1 mol) of p-ethylphenol, 7.2 g (0.1 mol) of 1,2-butylene oxide and 0.8 ml of a 50% aqueous solution of sodium hydroxide were heated at 140° to 145° C for 4 hours in the same way as in Example 1. The reaction mixture obtained was treated in the same way as in Example 1 to afford 14.8 g of 1-(p-ethylphenoxy)-butan-2-ol (compound No. 52) in a yield of 76.3%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04016186 |
| 출처 데이터셋 | uspto-grants-1977_04 |
| ORD ID | ord-92c1464e53d14e5f99903d078d027c3e |
| 출처 메모 | uspto-grants-1977_04 |