HRID328151

反应详情

EQUATION

反应方程式

HRID 328151 的结构方程式

PROCEDURE

实验过程

In a closed vessel 12.2g (0.1 mol) of p-ethylphenol, 7.2 g (0.1 mol) of 1,2-butylene oxide and 0.8 ml of a 50% aqueous solution of sodium hydroxide were heated at 140° to 145° C for 4 hours in the same way as in Example 1. The reaction mixture obtained was treated in the same way as in Example 1 to afford 14.8 g of 1-(p-ethylphenoxy)-butan-2-ol (compound No. 52) in a yield of 76.3%.

WORKUP

后处理

  1. customThe reaction mixture obtained
  2. additionwas treated in the same way as in Example 1