HRID328223

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID121052

[1,1'-Biphenyl]-2-carbaldehyde

C13H10O

HCID4599837

Carbamimidoyl-acetic acid ethyl ester

C5H10N2O2

PRODUCTS

生成物

结构：CCOC(=O)C1=C(N)NC(N)=C(C(=O)OCC)C1c1ccccc1-c1ccccc1

HCID70631644

未命名化合物

收率 33%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID702

Ethanol

C2H6O

2 次

PROCEDURE

实验过程

Upon heating a solution of 9.1 g biphenyl-2-aldehyde and 13.0 g amidinoacetic acid ethyl ester in 200 ml ethanol for two hours, 2,6-diamino-4-(biphenyl-2-yl)-1,4-dihydropyridine-3,5-dicarboxylic acid diethyl ester of m.p. 215° (ethanol) is obtained.