HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21441246, compound → HCID 21441250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21441246 | HCID 21441246 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21441250 | HCID 21441250 | — |
Reaction Steps
The crude ester is heated under reflux for 3 hours in 150 ml water and 100 ml 95% ethanol containing 20 g NaOH. The mixture is poured into water and the resulting solid removed by filtration, washed with water and air-dried to give 24.4 g crude 3-benzyloxy-6-methylphthalic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04017299 |
| Source dataset | uspto-grants-1977_04 |
| ORD ID | ord-b0782eb45d984b0ca30835b37108f45e |
| Source note | uspto-grants-1977_04 |